Fig. 3: Flame-synthesized nanocrystal MOF, Cu HKUST-1.
From: A general flame aerosol route to kinetically stabilized metal-organic frameworks
a Structural schematic, SEM, TEM images, and HAADF-STEM and STEM-EDS elemental maps; b XRD patterns of experimental and simulated Cu HKUST-1; c FTIR spectra of Cu(NO3)2, BTC ligand, and Cu HKUST-1; d 1H NMR spectrum. The MOF was digested in a mixture of 35% DCl in D2O and DMSO-d6; e N2 adsorption isotherm plot and Horvath–Kawazoe differential pore volume plot (60 mM Cu2+). Similar characterization results for additional nanocrystal MOFs are shown in Supplementary Figs. 6–9.
