Fig. 7: Scale-up experiments of PEC Cu-assisted BIOR. | Nature Communications

Fig. 7: Scale-up experiments of PEC Cu-assisted BIOR.

From: Direct generation of nitrogen-centered radicals via non-covalent interaction between Cu complexes and BiVO4 photoanodes

Fig. 7

a Photograph of the experimental setup in the gram-scale synthesis and the illustration of the two-electrode PEC flow reactor. b LSV curves of the scaled BiVO4 photoanodes measured in 0.2 M BI with 10 ppm Cu ions in a two-electrode cell. c The average photocurrent, yield rate and FE(BA) as a function of reaction time. d 1H and e 13C NMR spectra (400 MHz, CDCl3) of collected solid products. The insets were the photograph of separated product and its structure, respectively.

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