Scheme 2
Schematics of the experimental setup for the continuous-flow microwave-assisted synthesis of MOFs. The system comprises a reagent feed mechanism using syringe pumps, a tubular reactor positioned within a microwave cavity for uniform volumetric heating, and a back-pressure regulator to control system pressure. The configuration enables precise adjustment of flow rate, temperature, and residence time, facilitating rapid and scalable MOF crystallization under continuous operation. Reproduced from ref. 92. Copyright 2016, John Wiley & Sons.
