Extended Data Fig. 3: Precursor structure and its evolution during solid-state synthesis. | Nature Nanotechnology

Extended Data Fig. 3: Precursor structure and its evolution during solid-state synthesis.

From: Gas-mediated defect engineering in earth-abundant Mn-rich layered oxides for non-aqueous sodium-based batteries

Extended Data Fig. 3: Precursor structure and its evolution during solid-state synthesis.

(a) In situ SXRD patterns and (b) corresponding structural evolutions of Ni0.25Mn0.75CO3-NaOH mixture during solid-state calcination. The wavelength for the in situ heating SXRD measurement is 0.24108 Å. SXRD patterns acquired under continuous heating with no holding at fixed temperatures.

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