Table 2 Composition analyses for BiT-Bi and BiT-La. EDS data for grain composition were obtained by surface scans on five entire grains, and the mean value and standard deviation were listed.
Sample | elements | grain | Point 2 at grain boundary | theoretical composition |
|---|---|---|---|---|
BiT-Bi (Bi4Ti3O12 • 0.06Bi2O3) | O (at. %) | 63.44(0.38) | 66.77 | 63.11 |
Bi (at. %) | 21.36(0.41) | 20.15 | 21.35 | |
Ti (at. %) | 15.20(0.46) | 13.08 | 15.54 | |
BiT-La (Bi4Ti3O12 • 0.06La2O3) | O (at. %) | 63.34(0.45) | 65.24 | 63.11 |
Bi (at. %) | 20.83(0.32) | 20.55 | 20.73 | |
Ti (at. %) | 15.28(0.42) | 13.79 | 15.54 | |
La (at. %) | 00.55(0.21) | 00.43 | 0.62 |