Table 3 Yield at the prescribed RSM method.
Sl. no | KOH (%W/v) | Temperature (°C) | Molar ratio | Time (min) | Yield (%) |
|---|---|---|---|---|---|
1 | 1 | 55 | 10 | 120 | 54.57 |
2 | 0.5 | 45 | 8 | 60 | 90.34 |
3 | 1.5 | 45 | 12 | 180 | 89.35 |
4 | 1 | 75 | 10 | 120 | 88.79 |
5 | 1.5 | 65 | 8 | 60 | 78.33 |
6 | 0 | 55 | 10 | 120 | 76.1 |
7 | 1.5 | 45 | 12 | 60 | 76.21 |
8 | 0.5 | 65 | 8 | 60 | 86.18 |
9 | 1.5 | 65 | 12 | 60 | 82.77 |
10 | 1 | 55 | 10 | 240 | 74.32 |
11 | 1 | 55 | 6 | 120 | 94.62 |
12 | 0.5 | 45 | 12 | 60 | 76.21 |
13 | 1.5 | 45 | 8 | 180 | 75.26 |
14 | 1 | 55 | 10 | 120 | 63.27 |
15 | 0.5 | 65 | 12 | 180 | 92 |
16 | 2 | 55 | 10 | 120 | 66.73 |
17 | 0.5 | 45 | 12 | 180 | 57.68 |
18 | 1.5 | 65 | 12 | 180 | 65.89 |
19 | 1 | 55 | 14 | 120 | 54.56 |
20 | 1.5 | 45 | 8 | 60 | 76.06 |
21 | 1 | 55 | 10 | 120 | 92.5 |
22 | 1 | 55 | 10 | 120 | 91.92 |
23 | 1 | 35 | 10 | 120 | 95.69 |
24 | 0.5 | 65 | 8 | 180 | 76.27 |
25 | 1 | 55 | 10 | 120 | 73.56 |
26 | 1 | 55 | 10 | 0 | 89.59 |
27 | 1.5 | 65 | 8 | 180 | 76.33 |
28 | 0.5 | 65 | 12 | 60 | 51.26 |
29 | 0.5 | 45 | 8 | 180 | 96.32 |
30 | 1 | 55 | 10 | 120 | 80.35 |