Table 1 Spectrophotometric parameters for MIR determination with TAM.
Parameters | DW | RD | DD1 | ||||
|---|---|---|---|---|---|---|---|
MIR | TAM | MIR | TAM | MIR | TAM | ||
Range (µg/mL) | 3–20 | 2–40 | 3–20 | 2–40 | 3–20 | 2–40 | |
Determination coefficient | 0.9996 | 0.9998 | 0.9994 | 0.9997 | 0.9994 | 0.9998 | |
Slope | 0.03 | 0.02 | 5.86 | 0.42 | 0.61 | 0.05 | |
Intercept | − 0.03 | 0.01 | − 5.70 | 0.07 | − 0.61 | 0.008 | |
LOD (µg/mL) | 0.36 | 0.57 | 0.45 | 0.61 | 0.44 | 0.54 | |
LOQ (µg/mL) | 1.09 | 1.75 | 1.38 | 1.87 | 1.34 | 1.64 | |
Wavelength | 240–266 nm | 230–262 | 220–248 nm | 221–295 nm | 242 nm | 302 nm | |
Accuracy (Recovery%±SD) | 98.90 ± 0.75 | 100.12 ± 0.68 | 100.12 ± 0.42 | 99.97 ± 1.02 | 99.73 ± 0.38 | 99.17 ± 0.95 | |
Precision %RSD | Intraday | 0.55 | 0.45 | 0.65 | 0.53 | 0.28 | 0.94 |
Interday | 0.87 | 0.55 | 0.77 | 1.26 | 0.38 | 1.18 | |