Table 4 Chromatographic Method Robustness.
Drugs | Factor | Analyst to analyst | Column temperature oC | Flow rate (mL/min) | |||
|---|---|---|---|---|---|---|---|
Changes | 24,25,26 | 0.95,1,1.05 | |||||
Tested parameters | Peak area | Retention time | Peak area | Retention time | Peak area | Retention time | |
MIR | RSD% | 1.824 | 0.362 | 1.453 | 0.214 | 1.721 | 0.742 |
TAM | RSD% | 1.963 | 0.472 | 1.683 | 0.162 | 1.824 | 0.947 |