Fig. 5 | Scientific Reports

Fig. 5

From: Randomized-field microwave-assisted pharmaceutical lyophilization with closed-loop control

Fig.  5The alternative text for this image may have been generated using AI.

Experimentally measured temperatures and pressures for Cases SM1 and SM2 of Table 1, shown in (a, c) and (b, c) respectively. Lumped-capacitance model simulations are also shown in (a) and (b). \(T_\text {f1}\), \(T_\text {f2}\), and \(T_\text {f3}\) are product temperature readings in different center vials; \(T_\text {vw}\) is the temperature measured on the outside wall of a vial. Model curves terminate at predicted end of primary drying. In (a), the model \(R_{p}\) was adjusted to match product temperature readings. All microwave-related parameters are determined from Case M1 in Fig. 8 below, so Case SM2 in (b) has no tuning parameters.

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