Table 3 Experimental and predicted test matrix using CCD for CSLB preparation.
Std. order | Run order | MR: methanol/CSL molar ratio | PT: process temperature (°C) | IC: industrial catalyst (wt%) | CSLB yield (%) | ||
|---|---|---|---|---|---|---|---|
Experimental value | Predicted value | Residual | |||||
20 | 1 | 15 | 70 | 4 | 84.20 | 81.84 | 1.3 |
19 | 2 | 15 | 70 | 4 | 83.10 | 81.84 | -0.2 |
14 | 3 | 15 | 70 | 6 | 82.40 | 85.19 | 1.37 |
10 | 4 | 20 | 70 | 4 | 85.30 | 85.54 | -0.28 |
9 | 5 | 10 | 70 | 4 | 73.60 | 72.68 | 1.4 |
12 | 6 | 15 | 80 | 4 | 65.50 | 68.27 | 1.44 |
8 | 7 | 15 | 80 | 6 | 72.90 | 70.17 | -0.5 |
1 | 8 | 10 | 60 | 2 | 39.30 | 39.58 | -0.82 |
11 | 9 | 15 | 60 | 4 | 63.80 | 65.37 | 1.3 |
3 | 10 | 10 | 80 | 2 | 48.50 | 48.31 | 1.26 |
7 | 11 | 10 | 80 | 6 | 63.50 | 64.53 | -1.11 |
2 | 12 | 20 | 60 | 2 | 60.20 | 59.45 | -1.85 |
16 | 13 | 15 | 70 | 4 | 81.10 | 81.84 | -2.3 |
15 | 14 | 15 | 70 | 4 | 82.40 | 81.84 | -0.7 |
18 | 15 | 15 | 70 | 4 | 83.00 | 81.84 | 1.42 |
6 | 16 | 20 | 60 | 6 | 74.20 | 73.30 | -0.97 |
4 | 17 | 20 | 80 | 2 | 63.20 | 62.31 | -1.3 |
5 | 18 | 10 | 60 | 6 | 61.80 | 61.60 | -0.5 |
13 | 19 | 15 | 70 | 2 | 68.60 | 70.15 | 1.5 |
17 | 20 | 15 | 70 | 4 | 80.90 | 81.84 | -2.5 |