Abstract
Three-dimensional (3D) complementary metal–oxide–semiconductor (CMOS) integration could enable device scaling beyond the limits of conventional 2D CMOS technology. Such integration requires vertical electrical connections that pass through silicon substrates and interconnect stacked chips. The fabrication of these through-silicon vias (TSVs) creates new challenges in metrology, including the characterization of the thin isolation film deposited on the sidewalls of the TSVs and thickness characterization for wafer thinning. Here, we show that laser-induced terahertz emission microscopy can be used to characterize TSVs. Terahertz emission is observed through the excitation of a transient electric dipole in the depletion field of the TSV using femtosecond laser pulses. The detected terahertz waveform provides information about the local depletion field and thus structural information about the isolation film. By performing a time-of-flight measurement of the terahertz pulse, we can also extract the silicon wafer thickness.
This is a preview of subscription content, access via your institution
Access options
Access Nature and 54 other Nature Portfolio journals
Get Nature+, our best-value online-access subscription
$32.99 / 30 days
cancel any time
Subscribe to this journal
Receive 12 digital issues and online access to articles
$119.00 per year
only $9.92 per issue
Buy this article
- Purchase on SpringerLink
- Instant access to the full article PDF.
USD 39.95
Prices may be subject to local taxes which are calculated during checkout






Similar content being viewed by others
Data availability
The data that support the plots within this paper and other findings of this study are available from the corresponding author upon reasonable request.
References
Beyne, E. The rise of the 3rd dimension for system integration. In Proc. 2006 IEEE International Interconnect Technology Conference 1–5 https://doi.org/10.1109/IITC.2006.1648629 (IEEE, 2006).
Beyne, E. The 3-D interconnect technology landscape. IEEE Des. Test 33, 8–20 (2016).
Garrou, P., Bower, C. & Ramm, P. Handbook of 3D Integration: Technology and Applications of 3D Integrated Circuits (Wiley, 2008).
Gambino, J. P., Adderly, S. A. & Knickerbocker, J. U. An overview of through-silicon-via technology and manufacturing challenges. Microelectron. Eng. 135, 73–106 (2015).
Van der Plas, G. et al. Design issues and considerations for low-cost 3D TSV IC technology. In Proc. IEEE International Solid-State Circuits Conference (ISSCC) 148–149 (IEEE, 2010).
Croes, K. et al. Reliability challenges related to TSV integration and 3-D stacking. IEEE Des. Test 33, 37–45 (2016).
Li, Y. et al. Reliability challenges for barrier/liner system in high aspect ratio through silicon vias. Microelectron. Reliab. 54, 1949–1952 (2014).
Vartanian, V. H. et al. Metrology needs for through-silicon via fabrication. J. Micro/Nanolithogr. MEMS MOEMS 13, 011206 (2014).
Bender, H. et al. Structural characterization of through silicon vias. J. Mater. Sci. 47, 6497–6504 (2012).
Tonouchi, M. Simplified formulas for the generation of terahertz waves from semiconductor surfaces excited with a femtosecond laser. J. Appl. Phys. 127, 245703 (2020).
Teh, W. H., Marx, D., Grant, D. & Dudley, R. Backside infrared interferometric patterned wafer thickness sensing for through silicon-via (TSV) etch metrology. IEEE Trans. Semicond. Manuf. 23, 419–422 (2010).
Park, J., Jin, J., Kim, J. W. & Kim, J. A. Measurement of thickness profile and refractive index variation of a silicon wafer using the optical comb of a femtosecond pulse laser. Opt. Commun. 305, 170–174 (2013).
Ahn, H., Bae, J., Park, J. & Jin, J. A hybrid non-destructive measuring method of three-dimensional profile of through silicon vias for realization of smart devices. Sci. Rep. 8, 15342 (2018).
Katti, G. et al. Technology assessment of through-silicon via by using C–V and C–t measurements. IEEE Electron Device Lett. 32, 946–948 (2011).
Sze, S. M. & Ng, K. K. Physics of Semiconductor Devices (Wiley, 2007).
Nicollian, E. H. & Brews, J. R. MOS (Metal Oxide Semiconductor) Physics and Technology (Wiley, 2002).
Shen, Y. Surface properties probed by second-harmonic and sum-frequency generation. Nature 337, 519–525 (1989).
Murakami, H. & Tonouchi, M. Laser terahertz emission microscopy. C. R. Phys. 9, 169–183 (2008).
Murakami, H. et al. Scanning laser THz imaging system. J. Phys. D 47, 374007 (2014).
Hoyer, P., Theuer, M., Beigang, R. & Kley, E. B. Terahertz emission from black silicon. Appl. Phys. Lett. 93, 091106 (2008).
Philipp, H. R. & Taft, E. A. Optical constants of silicon in the region 1 to 10 ev. Phys. Rev. 120, 37–38 (1960).
Van Exter, M. & Grischkowsky, D. Optical and electronic properties of doped silicon from 0.1 to 2 THz. Appl. Phys. Lett. 56, 1694 (1990).
Maxwell, J. C. A dynamical theory of the electromagnetic field. Phil. Trans. R. Soc. Lond. 155, 459–512 (1865).
Dember, H. Über eine photoelektronische Kraft in Kupferoxydul-Kristallen. Z. Phys. 32, 554 (1931).
Zhang, X. & Auston, D. H. Optoelectronic measurement of semiconductor surfaces and interfaces with femtosecond optics. J. Appl. Phys. 71, 326 (1992).
Auston, D. H. Subpicosecond electro optic shock waves. Appl. Phys. Lett. 43, 713 (1983).
Gu, P., Tani, M., Kono, S., Sakai, K. & Zhang, X.-C. Study of terahertz radiation from InAs and InSb. J. Appl. Phys. 91, 5533 (2002).
Shibuya, T. et al. Terahertz-wave generation using a 4-dimethylamino-N-methyl-4-stilbazolium tosylate crystal under intra-cavity conditions. Appl. Phys. Exp. 1, 042002 (2008).
Mochizuki, T. et al. Probing the surface potential of oxidized silicon by assessing terahertz emission. Appl. Phys. Lett. 110, 163502 (2017).
Heyman, J. N., Coates, N., Reinhardt, A. & Strasser, G. Diffusion and drift in terahertz emission at GaAs surfaces. Appl. Phys. Lett. 83, 5476 (2003).
Wang, K. & Mittleman, D. M. Guided propagation of terahertz pulses on metal wires. J. Opt. Soc. Am. B 22, 2001–2008 (2005).
Jeona, T., Zhang, J. & Grischkowsky, D. THz Sommerfeld wave propagation on a single metal wire. Appl. Phys. Lett. 86, 161904 (2005).
Park, S., Hamh, S., Park, J., Kim, J. & Lee, J. Possible flat band bending of the Bi1.5Sb0.5Te1.7Se1.3 crystal cleaved in an ambient air probed by terahertz emission spectroscopy. Sci. Rep. 6, 36343 (2016).
Johnston, M. B., Whittaker, D. M., Corchia, A., Davies, A. G. & Linfield, E. H. Simulation of terahertz generation at semiconductor surfaces. Phys. Rev. B 65, 165301 (2002).
Matsudaira, A., Mehrotra, S. R., Ahmed, S. S., Klimeck, G. & Vasileska, D. MOSCap (2014); https://nanohub.org/resources/moscaphttps://doi.org/10.4231/D3736M30D
Burford, N. M. & El-Shenawee, M. O. Review of terahertz photoconductive antenna technology. Opt. Eng. 56, 010901 (2017).
Murakami, H., Takarada, T. & Tonouchi, M. Low-temperature GaAs-based plasmonic photoconductive terahertz detector with Au nano-islands. Photonics Res. 8, 1448–1456 (2020).
Murakami, H., Mizui, K. & Tonouchi, M. High-sensitivity photoconductive detectors with wide dipole electrodes for low frequency THz wave detection. J. Appl. Phys. 125, 151610 (2019).
Beyne, E. Reliable via-middle copper through-silicon via technology for 3-D integration. IEEE Trans. Compon. Packag. Manuf. Technol. 6, 983–992 (2015).
Acknowledgements
We acknowledge support from imec’s 3D integration team and industrially affiliated partners and thank I. Kawayama for fruitful discussions. K.J.P.J. is grateful to O. Wada for his encouragement and support of this work. This work was partially supported by a scientific research grant (PE18026) from the Japan Society for the Promotion of Science (JSPS), as well as the JSPS Core-to-Core Program and the FWO.
Author information
Authors and Affiliations
Contributions
This work was conceived jointly by K.J.P.J. and M.T. K.J.P.J. and F.M. conducted the experimental work. The experimental apparatus was designed by H.M. and constructed by K.S. and F.M. All authors discussed the results and wrote the manuscript.
Corresponding author
Ethics declarations
Competing interests
The authors declare no competing interests.
Additional information
Peer review information Nature Electronics thanks Richard Allen, Kubilay Sertel and the other, anonymous, reviewer(s) for their contribution to the peer review of this work.
Publisher’s note Springer Nature remains neutral with regard to jurisdictional claims in published maps and institutional affiliations.
Supplementary information
Supplementary Information
Supplementary Figs. 1 and 2.
Rights and permissions
About this article
Cite this article
Jacobs, K.J.P., Murakami, H., Murakami, F. et al. Characterization of through-silicon vias using laser terahertz emission microscopy. Nat Electron 4, 202–207 (2021). https://doi.org/10.1038/s41928-021-00559-z
Received:
Accepted:
Published:
Version of record:
Issue date:
DOI: https://doi.org/10.1038/s41928-021-00559-z
This article is cited by
-
Fast in-line failure analysis of sub-micron-sized cracks in 3D interconnect technologies utilizing acoustic interferometry
Communications Engineering (2024)


