Table 1 Data collection and refinement statistics

From: Characterization of exoribonuclease XRN1 as a cancer target and identification of adenosine-3’,5’-bisphosphate as a potent enzyme inhibitor

 

hXRN1x-pAp

Data Collection

Space group

P 21 21 21

Cell dimensions

 a, b, c (Å)

60.91, 63.97, 363.15

  α, β, γ (°)

90, 90, 90

 Resolution (Å)

48.00 - 2.10 (2.14-2.10)

 Rmerge

0.163 (1.200)

 I / σI

10.9 (2.1)

 CC1/2

0.998 (0.731)

 Completeness (%)

100.0 (100.0)

 Redundancy

13.1 (13.5)

Refinement

 Resolution (Å)

48.05 - 2.10 (2.154-2.100)

 No. reflections

79953 (5788)

 Rwork / Rfree

0.187 / 0.227

No. atoms

 Protein

9327

 Ligand/Mg ion

54/2

 Water

723

B-factors

 Protein

45.18

 Ligand/ion

34.50/52.03

 Water

42.54

R.m.s. deviations

 Bond lengths (Å)

0.0104

 Bond angles (°)

1.94

  1. Values in parentheses are for highest-resolution shell.
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