Extended Data Fig. 10: Understanding the acceleration rate and the effects of stage temperature, Ts, and solvent partial pressure PHFIP or PAcOH.

(a, d) Regression of the acceleration rates versus the synthesis conditions, that is, Ts and PHFIP or AcOH (to obtain the apparent activation energies and rate constants), where the orange dots in (a) denote the data obtained using HFIP and those in (d) denote the data obtained using AcOH. (b, e) Corresponding contour plots of the acceleration rate surface with the conditions that gave rise to the same acceleration rate connected by a contour line. (c, f) Linear correlation between the predicted acceleration rate and the values measured experimentally for HFIP and AcOH.