Fig. 3: Macro- and microstructural evolution during H2-based redox alloying. | npj Advanced Manufacturing

Fig. 3: Macro- and microstructural evolution during H2-based redox alloying.

From: Hydrogen-based ore-to-part manufacturing of near-net-shape stainless steel

Fig. 3: Macro- and microstructural evolution during H2-based redox alloying.

a X-ray diffractograms of the oxide mixture before and after H2-based redox alloying in the tube furnace. b Photographs showing the geometrical changes of the gal-cast part. c Comparison between theoretical shrinkage calculated from oxide reduction and the experimentally measured value. d Optical micrograph (left) and SEM-EDS maps (right) showing the dense microstructure decorated by Al- and Si-based particulates.

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