Fig. 5: Hydrolysis of amide products.
From: Ritter-type amination of C(sp3)-H bonds enabled by electrochemistry with SO42−
a Conditions: Amide compound (3.0 mmol, 1 eq.), NaOH (24 mmol, 8 eq.), 1-butanol as solvent, 130–135 °C for 7 h. Then, the free base was added 5 M aq. HCl (3 mL) to give hydrochloride. b Conditions: 25 (3.0 mmol, 1 eq.), HCl (3 M, 10 eq.), reflux for 3 h.
