Fig. 6: Mechanistic studies.
From: Ritter-type amination of C(sp3)-H bonds enabled by electrochemistry with SO42−
a Control experiments. aFor the reaction, to the anodic chamber was added 1a (0.5 mmol), H2SO4 (108 μL, 2 mmol, 0.67 M), nBu4NBF4 (0.1 M) and CH3CN (3 mL), the cathodic chamber was added nBu4NBF4 (0.1 M) and CH3CN (3 mL). b Radical trapping experiments. c Proposed mechanism.
