Fig. 2: MOF in-situ reconstruction. | Nature Communications

Fig. 2: MOF in-situ reconstruction.

From: Residual ligand-functionalized ultrathin Ni(OH)2 via reconstruction for high-rate HO2− electrosynthesis

Fig. 2: MOF in-situ reconstruction.

a Time-dependent XRD patterns of PR-utn-NiBDC. b pH-dependent XRD patterns of PR-utn-NiBDC. c Time-dependent XRD patterns of utn-NiBDC in 0.1 M KOH. Elemental mapping of d Cl-utn-NiBDC, e Cl-utn-NiBDC+KOH, and f Cl-utn-NiBDC+KOH for 12 h. g Raman, h FT-IR, and i high-resolution Ni 2p XPS spectra of utn-NiBDC, PR-utn-NiBDC, utn-NiBDC+KOH, and Ni(OH)2. Source data for Fig. 2a–c and Fig. 2g–i are provided as a Source Data file.

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