Fig. 4: Spectroscopic characterization of 2D IrO2(101) monolayer.

a XRD curves and b XPS spectra of IrO2(101) monolayer, IrO2 NP and Comm IrO2(Alfa Aesar), respectively. c Ir 4 f XPS spectra and d O 1 s XPS spectra of IrO2(101) monolayer and Comm IrO2(Alfa Aesar). e Raman spectra of IrO2(101) monolayer, IrO2 NP and Comm IrO2(Alfa Aesar). f Nitrogen adsorption-desorption isotherms of IrO2(101) monolayer, IrO2 NP and Comm IrO2(Alfa Aesar).