Abstract
Electron beam melting (EBM) is an additive manufacturing technology that can process materials and manufacture components otherwise impossible or uneconomical. However, defects, including porosity and surface irregularities, are widely reported in EBM-built components, and their formation mechanisms are not fully understood. Here, using in-situ high-speed synchrotron X-ray imaging, we reveal that bubble explosions in Al6061 during EBM induce melt pool instabilities contributing to defect formation. The melt pool and keyhole evolve through three stages: (1) initial formation of a melt pool, (2) subsurface bubble formation and explosion, and (3) periodic keyhole oscillation. During scanning, periodic bubble explosions can eject molten liquid as spatters and disturb the vapor depression and melt pool, contributing to surface humping, that may trigger lack-of-fusion defects in subsequent layers. The physical insights we report could provide guidance for EBM machine development, process innovation, alloy design and model development.
Data availability
The authors declare that the data supporting the findings of this study are available within the paper and its supplementary information files Source data are provided with this paper.
References
Lodes, M. A., Guschlbauer, R. & Körner, C. Process development for the manufacturing of 99.94% pure copper via selective electron beam melting. Mater. Lett. 143, 298–301 (2015).
Sharabian, E., Leary, M., Fraser, D. & Gulizia, S. Electron beam powder bed fusion of copper components: a review of mechanical properties and research opportunities. Int. J. Adv. Manuf. Technol. 122, 513–532 (2022).
Dadbakhsh, S. et al. Process and geometrical integrity optimization of electron beam melting for copper. CIRP Ann 71, 201–204 (2022).
Ledford, C. et al. Evaluation of electron beam powder bed fusion additive manufacturing of high-purity copper for overhang structures using in-situ real-time backscatter electron monitoring. Procedia Manuf. 48, 828–838 (2020).
Lu, L. et al. Impact response of a high-Nb TiAl alloy fabricated via electron beam melting. J. Alloys Compd. 1014, 178556 (2025).
Ramsperger, M., Singer, R. F. & Körner, C. Microstructure of the Nickel-base superalloy CMSX-4 fabricated by selective electron beam melting. Metall. Mater. Trans. A 47, 1469–1480 (2016).
Kolbus, L. et al. Comparison of residual stresses in Inconel 718 simple parts made by electron beam melting and direct laser metal sintering. Metall. Mater. Trans. A 46, 1419 (2015).
Wensrich, C. M., Luzin, V., Hendriks, J. N., Pant, P. & Gregg, A. W. T. Residual stress in additively manufactured Inconel cubes; selective laser melting versus electron beam melting and a comparison of modelling techniques. Mater. Des. 244, 113108 (2024).
Anwar, S. et al. On the turning of electron beam melted gamma-TiAl with coated and uncoated tools: a machinability analysis. J. Mater. Process. Technol. 282, 116664 (2020).
Wang, L. et al. Defects, microstructure and properties in additive manufacturing of TiAl alloys: Formation mechanisms, influencing factors and improvement strategies. Mater. Des. 256, 114235 (2025).
Dorow-Gerspach, D. et al. Additive manufacturing of high-density pure tungsten by electron beam melting. Nucl. Mater. Energy 28, 101046 (2021).
Fernandez-Zelaia, P. et al. Crystallographic texture evolution in electron beam melting additive manufacturing of pure molybdenum. Mater. Des. 207, 109809 (2021).
Di Sturco, S. et al. Understanding the processability, microstructure, and mechanical properties of molybdenum processed by electron beam powder bed fusion. Int. J. Refract. Met. Hard Mater. 129, 107091 (2025).
Ellis, E. A. I. et al. Processing of tungsten through electron beam melting. J. Nucl. Mater. 555, 153041 (2021).
Philips, N., Rock, C., Cunningham, N., Cooper, J. & Horn, T. Electron beam powder bed fusion of ATI C103TM refractory alloy. Metall. Mater. Trans. A 55, 2472–2484 (2024).
Westrich, Y., Kammermeier, E., Wahlmann, B. & K”rner, C. Three-dimensional spot melting patterns in electron beam powder bed fusion: high efficiency and tailored texture. Prog. Addit. Manuf. 10, 10549–10562 (2025).
Khrenov, M., Templeton, W. F. & Narra, S. P. Addopt: An additive manufacturing optimal control framework demonstrated in minimizing layer-level thermal variance in electron beam powder bed fusion. J. Manuf. Sci. Eng. 147, 041009 (2025).
Shi, Y. et al. Electron beam metal additive manufacturing: defect formation and in-process control. J. Manuf. Process. 101, 386–431 (2023).
Polonsky, A. T. et al. Defects and 3D structural inhomogeneity in electron beam additively manufactured Inconel 718. Mater. Charact. 143, 171–181 (2018).
Fu, Z. & Körner, C. Actual state-of-the-art of electron beam powder bed fusion. Eur. J. Mater. 2, 54–116 (2022).
Guo, C., Ge, W. & Lin, F. Effects of scanning parameters on material deposition during electron beam selective melting of Ti-6Al-4V powder. J. Mater. Process. Tech. 217, 148–157 (2015).
Juechter, V., Scharowsky, T., Singer, R. F. & Ko, C. Processing window and evaporation phenomena for Ti-6Al-4V produced by selective electron beam melting. Acta Mater 76, 252–258 (2014).
Lin, Z., Dabakhsh, S. & Rashid, A. Developing processing windows for powder pre-heating in electron beam melting. J. Manuf. Process. 83, 180–191 (2022).
Narra, S. P., Cunningham, R., Beuth, J. & Rollett, A. D. Location-specific solidification microstructure control in electron beam melting of Ti-6Al-4. V. Addit. Manuf. 19, 160–166 (2018).
Ye, J., Semjatov, N., Bidola, P., Lindwall, G. & Körner, C. Revealing the mechanisms of smoke during electron beam–powder bed fusion by high-speed synchrotron radiography. J. Manuf. Mater. Process. 8, 103 (2024).
Chauvet, E. et al. Hot cracking mechanism affecting a non-weldable Ni-based superalloy produced by selective electron beam melting. Acta Mater 142, 82–94 (2018).
Mostafaei, A. et al. Defects and anomalies in powder bed fusion metal additive manufacturing. Curr. Opin. Solid State Mater. Sci. 26, 100974 (2022).
DebRoy, T. et al. Additive manufacturing of metallic components – Process, structure and properties. Prog. Mater. Sci. 92, 112–224 (2018).
Yan, W. et al. Multi-physics modeling of single/multiple-track defect mechanisms in electron beam selective melting. Acta Mater 134, 324–333 (2017).
Yan, W. et al. Meso-scale modeling of multiple-layer fabrication process in selective electron beam melting: inter-layer/track voids formation. Mater. Des. 141, 210–219 (2018).
Kenevisi, M. S. & Lin, F. Effect of powder characteristics on relative density and porosity formation during electron beam selective melting of Al2024 aluminum alloy. J. Manuf. Sci. Eng. 145, 054501 (2023).
Yuan, J. et al. In-situ characterization of defect formation and elimination dynamics during electron beam melting using high-speed X-ray imaging. Addit. Manuf. Lett. 11, 100239 (2024).
Yim, S., Lee, T., Yanagihara, K., Aoyagi, K. & Yamanaka, K. Unveiling the influence of printing surfaces in powder bed fusion electron beam melting through multiphysics simulation. Addit. Manuf. 102, 104738 (2025).
Semjatov, N., Wahlmann, B. & Carolin, K. Multiple interaction electron beam powder bed fusion for controlling melt pool dynamics and improving surface quality. Addit. Manuf. 90, 104316 (2024).
Semjatov, N. et al. In-situ synchrotron imaging of powder consolidation and melt pool dynamics in electron beam powder bed fusion. Addit. Manuf. 110, 104943 (2025).
Ge, W., Han, S., Fang, Y., Cheon, J. & Na, S. J. Mechanism of surface morphology in electron beam melting of Ti6Al4V based on computational flow patterns. Appl. Surf. Sci. 419, 150–158 (2017).
Hojjatzadeh, S. M. H. et al. Direct observation of pore formation mechanisms during LPBF additive manufacturing process and high-energy-density laser welding. Int. J. Mach. Tools Manuf. 153, 103555 (2020).
Huang, Y. et al. Keyhole fluctuation and pore formation mechanisms during laser powder bed fusion additive manufacturing. Nat. Commun. 13, 1170 (2022).
Wassermann, N. A. et al. Evolution of powder-entrapped pores in Ti–6Al–4V fabricated with powder bed fusion-laser beam process. Addit. Manuf. 109, 104838 (2025).
Leung, C. L. A. et al. In situ X-ray imaging of defect and molten pool dynamics in laser additive manufacturing. Nat. Commun. 9, 1355 (2018).
Bhatt, A. et al. In situ characterisation of surface roughness and its amplification during multilayer single-track laser powder bed fusion additive manufacturing. Addit. Manuf. 77, 103809 (2023).
Wolff, S. J. et al. In situ X-ray imaging of pore formation mechanisms and dynamics in laser powder-blown directed energy deposition additive manufacturing. Int. J. Mach. Tools Manuf. 166, 103743 (2021).
Yan, W., Smith, J., Ge, W., Lin, F. & Kam, W. Multiscale modeling of electron beam and substrate interaction: a new heat source model. Comput. Mech. 56, 265–276 (2015).
Klassen, A., Bauereiß, A. & Körner, C. Modelling of electron beam absorption. J. Phys. D Appl. Phys. 065307, 065307 (2014).
Escano, L. I. et al. An electron beam melting system for in-situ synchrotron X-ray monitoring. Addit. Manuf. Lett. 3, 100094 (2022).
Cunningham, R. et al. Keyhole threshold and morphology in laser melting revealed by ultrahigh-speed x-ray imaging. Science 363, 849–852 (2019).
Guo, Q. et al. Transient dynamics of powder spattering in laser powder bed fusion additive manufacturing process revealed by in-situ high-speed high-energy x-ray imaging. Acta Mater 151, 169–180 (2018).
Heine, V. & Chen, S. Understanding metal bonding. J. Phys. Conf. Ser. 36, 353002 (2024).
Rutherford, E. The scattering of α and β particles by matter and the structure of the atom. Philos. Mag. J. Sci. 21, 669–688 (1911).
Armstrong, C. D., Brenner, C. M., Zemaityte, E., Klarenaar, B. L. M. & Guaitella, O. A Monte Carlo calculation on the scattering of electrons in copper. Proc. Phys. Soc. 85, 855 (1965).
Carlo, M. A Monte Carlo code to simulate the effect of fast secondary factors and spatial resolution in the TEM electrons on kAB. J. Microsc. 168, 153–167 (1992).
Aurégan, T. & Deike, L. Drainage and lifetime of thin liquid films: the role of salinity and convective evaporation. J. Fluid Mech. 1012, A18 (2025).
Nguyen, C. T. et al. Film drainage and the lifetime of bubbles. Geochem. Geophys. Geosyst. 14, 3616–3631 (2013).
Wang, D., Zhao, D., Liang, X., Li, X. & Lin, F. Multiple stages of smoking phenomenon in electron beam powder bed fusion process. Addit. Manuf. 66, 103434 (2023).
Qu, M. et al. Mitigating keyhole pore formation by nanoparticles during laser powder bed fusion additive manufacturing. Addit. Manuf. Lett. 3, 100068 (2022).
Zhao, C. et al. Critical instability at the moving keyhole tip generates porosity in laser melting. Science 370, 1080–1086 (2020).
Guo, Q. et al. In-situ full-field mapping of melt flow dynamics in laser metal additive manufacturing. Addit. Manuf. 31, 100939 (2020).
Qu, M. et al. Controlling melt flow by nanoparticles to eliminate surface wave-induced surface fluctuation. Addit. Manuf. 59, 103081 (2022).
Schneider, C. A., Rasband, W. S. & Eliceiri, K. W. NIH Image to ImageJ: 25 years of image analysis. Nat. Methods 9, 671–675 (2012).
Yuan, J. et al. Revealing mechanisms of processing defect mitigation in laser powder bed fusion via shaped beams using high-speed X-ray imaging. Int. J. Mach. Tools Manuf. 204, 104232 (2025).
Acknowledgments
This work is supported by Vilas Associate Award (L.C.) and the U.S. Department of Commerce (Award ID number: 70NANB21H039, L.C.). This research used resources of the Advanced Photon Source, a U.S. Department of Energy (DOE) Office of Science user facility operated for the DOE Office of Science by Argonne National Laboratory under Contract No. DE-AC02-06CH11357. The authors would like to thank Drs. Fan Zhang, Lyle Levine, Brandon Lane, Brian Simonds, and Nik Hrabe from the National Institute of Standards and Technology (NIST) for fruitful discussions. The authors appreciate Drs. Scott Sanders, Matthias Beuting, Brandon Walker and Kevin Eliceiri at the University of Wisconsin-Madison for their helpful suggestions.
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L.C. and J.Y. conceived the idea. L.C. supervised the research project. J.Y. and L.C. designed the experiment. L.I.E. S.J.C., K.F., J.Y., J.H., A.N., Q.L., and L.C. conducted the X-ray imaging experiments. J.Y. performed the data analysis and characterization. J.Y. and L.C. wrote the paper with input from all authors. All authors discussed the results and reviewed the manuscript.
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Nature Communications thanks Feng Lin, Nick Semjatov, and the other anonymous reviewer(s) for their contribution to the peer review of this work. A peer review file is available.
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Yuan, J., Escano, L.I., Clark, S.J. et al. Bubble explosion induced melt pool instabilities in electron beam melting of aluminum alloy. Nat Commun (2026). https://doi.org/10.1038/s41467-026-71118-3
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DOI: https://doi.org/10.1038/s41467-026-71118-3