Abstract
In this study, the effects of machining parameters on material removal rate (MRR), electrode wear rate (EWR) and surface roughness (Ra) in the electrical discharge machining (EDM) of nickel-chromium-based alloy were investigated. Discharge current (I), pulse-on time (Ton), pulse-off time (Toff) and graphite powder concentration were selected as variable parameters in the study. An experimental setup was designed and manufactured for use in powder-mixed EDM experiments. Mathematical models were generated using response surface methodology (RSM), the most effective parameters on the results were determined and regression equations were obtained. Parameter optimization was performed with the highest MRR, lowest EWR, and lowest Ra performance targets. The ideal machining conditions were determined as I = 12.5 A, Ton=66µs, Toff=6µs and powder-mixed dielectric. Using the powder-mixed dielectric, 34.54% higher MRR, 20.01% lower EWR and 12.64% lower Ra were achieved on average. Using the created mathematical model, the result of the machining to be done with these parameters was predicted and the reliability of the model was tested by comparing the predicted results of the model and the results of the verification experiment.
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Introduction
The effects of powder-mixed (PM) dielectrics on electrical discharge machining (EDM) have been studied by many researchers. Jeswani reported that the addition of graphite powder to dielectric fluid increased MRR by 60%, EWR by 15%, and decreased the MRR/EWR ratio by 28% in machining with a steel workpiece and copper electrode1. Kansal et al. showed that when silicon powder-mixed dielectric was used in the machining of EN-31 tool steel workpiece, improvement in MRR and Ra was achieved. powder concentration and I were the most effective parameters according to ANOVA results2. Kung et al. reported that the effect of aluminium powder addition on the MRR and EWR in machining of tungsten carbide workpiece increased as particle size, I and Ton increased; MRR increased up to a powder concentration of 15 g/l and then decreased, while the EWR decreased up to a powder concentration of 15 g/l and then increased3. Kumar and Davim emphasized that the use of silicon powder additive in EDM machining of Al-SiC composite increased the MRR by three times and reduced Ra by one-third, and that the most effective variables in this process were powder concentration and current4. Bhattacharya et al. performed machining on mould steels with different electrodes (copper, copper-tungsten) and powder additives (graphite, aluminium). The highest MRR was obtained with aluminium powder. They emphasized that the graphite powder additive reduced MRR and Ra, and that the effect of the electrode material on the outputs was weak5. Singh and Yeh modelled the machining of aluminium matrix composites using the GRA method. They reported that the most effective machining parameters were Ton, electrode retraction time, and powder size. Coarser powders decreased MRR and increased Ra. When machining was done with ideal parameters, MRR increased from 0.4267 to 0.530 g/min, EWR decreased from 0.0112 to 0.0096 g/min, and Ra decreased from 3.64 to 2.82 μm6. Assarzadeh and Ghoreishi modelled the machining of CK45 steel using RSM, finding that I and Ton were the most influential parameters on MRR, while I was the most influential on Ra. Increasing the voltage decreased MRR. The researchers calculated the maximum error rate of the developed model as 10.71% for MRR and 8.41% for Ra7. Jabbaripour et al. compared the effect of different powder additives (aluminium, graphite, SiC, chromium, and iron) on the machining of titanium aluminide material and stated that aluminium powder provided the highest MRR and the lowest Ra8. Singh et al. reported that the use of graphite powder -mixed dielectric in the machining of Superco 605 alloy reduced Ra, and that Ra increased as I increased. The researchers determined the ideal machining parameters to be I = 9 A and Ton=20µs, as identified through Taguchi analysis, which improved Ra from 2.23 to 1.99 μm9. Talla et al. modelled the EDM of aluminium-alumina composite using the GRA method, calculated the ideal machining parameters as I = 3 A and Ton=150µs, and reported that aluminium powder additive provided positive effects on both MRR and Ra10. Ünses and Çoğun stated that graphite powder addition increased MRR and decreased Ra in the machining of Ti-6Al-4 V alloy, but EWR also increased11. Long et al. achieved a 32.1% improvement in MRR when using 10 g/l titanium powder additive in EDM of various die steels12. S. Tripathy and D. K. Tripathy determined the ideal machining parameters for the chromium powder-mixed EDM of H-11 die steel as Cp=6 g/l, I = 6 A, Ton=100µs by the GRA method and Cp=6 g/l, I = 3 A, Ton=150µs by the TOPSIS method. Desirability of the outputs improved by 16.17% and 25.93%, respectively13. Mohal and Kumar stated that carbon nanotube addition increased MRR and decreased Ra in the EDM of Al-SiC material. As a result of RSM analysis, 38.22% improvement in MRR and 46.04% improvement in Ra were achieved. I was determined to be the most effective parameter on machining14. Banh et al. reported that increasing the titanium powder additive from 2 g/l to 6 g/l in the machining of die steels increased the MRR by 68%, reduced the EWR by 28% and improved the Ra15. Mohanty et al. modelled the EDM of Al-SiC material with RSM and showed that the powder additive had a positive effect on MRR and Ra by increasing the spark gap16. Jadam et al. reported that 0.5 g/l carbon nanotube addition increased MRR by 44.95%, decreased EWR by 64.1% and Ra by 14.1% in the machining of Inconel 718 alloy17. Sahu and Datta reported that graphite addition increased MRR by 13.08%, decreased EWR by 92.68% and Ra by 49.15% in the EDM machining of Inconel 718 alloy, and all three outputs increased with increasing I18. Alhodaib et al. performed GRA analysis on the silicon powder-mixed EDM of Nimonic-90 alloy, calculated the ideal machining parameters as Cp=12 g/l, I = 3 A, Ton=35µs and Toff=49µs, and achieved 50.04% improvement in Ra19. Ramesh and Jenarthanan modelled the machining of Nimonic alloy with various powder mixtures (graphite, silicon, manganese) using RSM and determined the ideal machining parameters as 3 g/l manganese powder, I = 3 A, 90% duty cycle. They determined the error rate of the generated model to be at most 6% and stated that the highest MRR was obtained with silicon and the lowest Ra was obtained with graphite powder20. Chakraborty et al. compared efficiency of two different methods, namely RSM and GRA-PCA for modelling WEDM of Ti6Al4V alloy. Optimum machining parameters were found as Ton=30µs, Toff=11µs, I = 1 A, Cp=2 g/l by RSM and outputs were 1.384 μm surface roughness and 8042 µm2 corner inaccuracy. Optimum machining parameters found by GRA-PCA were Ton=30µs, Toff=2µs, I = 3 A, Cp=4 g/l and outputs were 1.315 μm surface roughness and 11,623 µm2 corner inaccuracy. They reported that GRA-PCA method was better for modelling this process due to having a lower error rate of 3.94%, compared to 4.78% error rate of RSM model, and achieving lower Ra21. In further studies, Chakraborty et al. used Teaching and Learning Based Optimization technique in addition to RSM to model WEDM of Ti6Al4V. They found optimum machining parameters to be Ton=30.23µs, Toff=3.02µs, V = 79.9 V, Cp=3.1 g/l and outputs were found as 1.199 μm surface roughness and 12982.67 µm2 corner inaccuracy. They stated that usage of powder additive improved surface quality by 50.77% and corner accuracy by 23.01%22. Le et al. investigated the machinability of SKD61 steel in tungsten carbine powder mixed EDM. Researchers selected I, Ton and Cp as variable parameters and used reverse polarity copper electrodes. They determined optimal inputs as I = 1 A, Ton=30µs, Cp=13.6 g/l by DA, I = 1 A, Ton=20µs, Cp=20/l by TOPSIS and I = 1 A. It was stated that DA provided better EWR (0.000119419 g/min and 41.5% reduction) and better MRR (0.0013641 g/min and 22.7% increase) while TOPSIS provided better Ra (0.9326 μm and 13.89% reduction) and better surface quality (lesser number of crack and thinner recast layer). It was also emphasized that I had the highest effect on all three output parameters while Cp contributed least to MRR while Ton contributed the least to EWR and Ra23. In another study by Le et al., effects of machining parameters (I, Ton, Cp, electrode material) on MRR, EWR and surface features were investigated in PMEDM of X40CrMoV51 steel. I was reported that 121.35% higher MRR and 46.08 lower EWR was achieved with graphite electrode, however copper electrode provided 12.52% lower recast layer thickness and a better surface uniformity24. This study aimed to determine the optimum machining parameters for EDM of a nickel-based dental alloy, to achieve high MRR, low EWR and low Ra and to determine the effects of graphite powder additives on machining. The study used the “remanium® CSE” alloy, which had not previously been machined using EDM. It was aimed to show that EDM can be used as an alternative method in the high precision machining of this alloy. EDM is one of the most common unconventional manufacturing methods, allowing for the machining of materials with high surface hardness. Its advantages, such as the absence of mechanical contact and its suitability for machining complex 3D geometries, make it widely used in the mould-making, automotive and aerospace industries25. In this study, both graphite powder-mixed and non-powder mixed EDM experiments were conducted using copper electrodes. A special experimental setup consisting of a dielectric tank, a circulation pump, and a sprayer was designed and used for the powder-mixed EDM experiments. Graphite powder concentration, I, Ton, and Toff were set as variable parameters in the experiments, while open circuit and discharge voltages were kept constant. MRR, EWR, and Ra were measured. The findings and the effects of the parameters were evaluated using analysis of variance (ANOVA). Furthermore, a mathematical model was developed using response surface methodology (RSM), and ideal parameters were determined; the reliability of the model was then tested.
Experimental method
A Furkan Kompakt 1 Z-NC model electrical discharge machine was used in the study. A test setup was designed and manufactured for use in graphite powder-mixed EDM experiments (Fig. 1). The setup consists of a dielectric tank, a circulation pump, two valves, and two sprayers. The dielectric tank is made of polypropylene for chemical corrosion resistance, and its side surfaces are angled to prevent graphite powder from settling on the tank bottom. The circulation pump circulates the dielectric fluid. One valve was installed at the lowest point of the system to drain the dielectric fluid in the tank after the machining was done. The other valve was located between the pump and the sprayers, and the dielectric flushing pressure was adjusted using this valve. One of the sprayers was used to maintain dielectric circulation within the tank. In contrast, the other was used to continuously supply the graphite powder-mixed dielectric fluid into the spark gap.
Kerosene was used as the dielectric fluid in the study, and 12.5 g/L graphite powder was mixed into the dielectric fluid in powder-mixed EDM experiments. The reasons for using graphite powder were that studies have shown that it increases conductivity, which has positive effects on machining speed and surface quality, and that it is well suspended in the dielectric fluid11. A nickel-based alloy called “remanium® CSE” was selected as the workpiece material (Fig. 2a, b). A copper electrode was used in the study due to copper’s high electrical and thermal conductivity26. A chemical composition of nickel-based alloy is as shown in Table 1.
In the experiments, I, Ton, Toff and powder concentration were selected as variable parameters shown in Table 2. The machining depth was 2 mm, the open-circuit voltage was 130 V, the discharge voltage was 70 V, and the retraction distance was 2 mm; these settings were kept constant throughout the experiments. In all experiments, the workpiece was polarized positively and the electrode was polarized negatively. The I value used in the experiments were determined as 3, 6, and 12.5 A; the Ton values were 24, 48, and 99 µs; and the Toff values were 6, 12, and 24 µs. A total of 18 experiments were conducted.
Before and after each experiment, the workpiece and electrode used were weighed using a precision balance with a precision of 0.005 g, and MRR and EWR values were calculated by dividing the volumetric reduction by the machining time (Eqs. 1,2) and shown in Table 3. Further, the comparison of powder-mixed and non-powder-mixed EDM results is depicted in Table 4.
After the experiment, the surface roughness of each workpiece was measured using the Mitutoyo Surftest SJ-310 surface roughness tester. The measuring standard was set to ISO 1997, profile = R, cutting values λc = 0.8 μm and λs = 2.5 μm, sampling length = 5 mm, traverse speed = 0.5 mm/s, and spacing = automatic.
Mathematical modelling
Response Surface Methodology (RSM) was used in mathematical modelling and optimization of the experimental results. The general formula of RSM for quadratic polynomials is given in Eq. 1.
The \(\:{\beta\:}_{0}\) term represents the initial state of all variables, the \(\:{\beta\:}_{i}\) term represents linear relationships, the \(\:{\beta\:}_{ii}\) term represents quadratic relationships, and the \(\:{\beta\:}_{ij}\) term represents binary relationships. The coefficients of the regression equation are then obtained by applying the least squares method7.
Mathematical modelling of MRR
RSM analysis was performed for the graphite powder concentration, I, Ton, and Toff inputs, and the MRR output. The graphite powder concentration input was selected as categorical, while the other three inputs were selected as continuous. Variance analysis was then performed to determine the magnitude of the inputs’ impact on the results. The F value in the variance analysis table indicates the effect of the parameter on the results. A larger F value indicates that the parameter has a greater impact on the outcome. The P value indicates the statistical significance of the parameter. Parameters with a P value of “zero” are the most significant parameters and must be included in the regression equation. Parameters with a P value greater than 0.05 have a low impact on the regression equation and can safely be eliminated from the equation27. The R-sq value represents the percentage of variation in the value calculated by the model. The R-sq(adj) value is the adjusted R-sq value, which is the percentage of variation in the results obtained by the model adjusted for the number of independent variables in the equation. R-sq(adj) is more effective than R-sq in indicating the reliability of regression equations with a large number of independent variables. R-sq and R-sq(adj) values close to 100% indicate high model reliability28. Table 5 shows the variance analysis results of the mathematical model created for MRR.
To increase the reliability of the model, terms with high P values were removed. The “Toff” term was not removed from the model despite its high P value because it is a direct experimental parameter. The results of the new analysis of variance are presented in Table 6.
Table 6 shows that the most influential parameters on MRR are I, Ton, I*Ton and graphite powder concentration, respectively. The Toff parameter has an insignificant effect on MRR. Two regression equations were created: one for the powder-mixed dielectric and the other for the dielectric without the powder additive. The equations are given in Eq. 2 and Eq. 3.
Figure 3 shows the normal probability plot of the model created for MRR. In this plot, the red line represents the regression equation, the blue dots represent the experimental results, and the graph demonstrates the equation’s compatibility with the experimental results. The horizontal axis represents the difference between the model’s calculated value and the experimental data, and the vertical axis represents the percentage distribution.
Mathematical modelling of EWR
Then, RSM analysis was performed for EWR using the same inputs selected for MRR. The performance outputs and variance analysis results of the generated model are given in Table 7.
To increase the reliability of the model, values with high P values were removed. The results of the new analysis of variance are presented in Table 8.
Table 8 shows that the most effective parameters on EWR are I, I*Toff, I*Ton and Toff, respectively. The effects of Ton and powder concentration on EWR are insignificant. Two regression equations were created: one for the dielectric with powder additive and the other for the dielectric without powder additive. The equations are given in Eq. 4 and Eq. 5.
Figure 4 shows the normal probability graph of the model created for EWR.
Mathematical modelling of Ra
Finally, RSM analysis was performed for Ra using the same inputs selected for MRR. The performance outputs and variance analysis results of the generated model are given in Table 9.
To increase the reliability of the model, values with high P values were removed. The results of the new variance analysis are given in Table 10.
As seen in Table 10, the most influential parameter on Ra is I, followed by I2, I*Ton, powder concentration, I*Toff and Ton. The effect of Toff on Ra is insignificant. Two regression equations were created: one for the dielectric with powder additive and the other for the dielectric without powder additive. The equations are given in Eq. 6 and Eq. 7.
The normal probability graph of the model created for Ra is given in Fig. 5.
Discussion of experimental results
Main effects plots were created to determine the linear effects of machining parameters on the results. Figure 6 shows that MRR increases as I and Ton increase, while MRR decreases as Toff increases. As I increases, the discharge energy increases, and as Ton increases, discharges last longer. These two factors cause each discharge to remove a larger volume of material from the workpiece. No machining occurs during Toff29. The results are consistent with theoretical data. The use of powder-mixed dielectric has been shown to increase MRR. The use of a powder-mixed dielectric has a positive effect on MRR by facilitating electrical discharge and shortening spark delay.
Figure 7 shows that EWR decreases as Ton increases and it increases as I, Toff increase. As I increases, discharge energy increases, which results in greater material erosion from the electrode as well as the workpiece. When Ton is kept short, heat does not spread throughout the electrode but remains only in the spark zone. However, when Ton is increased, thanks to copper’s good thermal conductivity, heat spreads throughout the electrode, reducing the heat accumulated on the surface in contact with the workpiece. Furthermore, because more material erosion occurs with a single discharge at longer Ton values, the total number of discharges during machining is reduced29. It is thought that this is why the EWR decreases when I is decreased and Ton is increased. Lower EWR has been obtained with the powder-mixed dielectric but ANOVA results show that effect of using powder mixed dielectric was insignificant on this parameter.
Figure 8 shows that Ra first increases and then decreases as I increases and that it increases as Ton and Toff increase. Lower Ra values have been obtained by using powder mixed dielectric. This is more evident in machining experiments conducted with high I.
Optimization of parameters and verification experiment
Parameter optimization was performed after obtaining regression equations for all three performance outcomes. Minimum Ra, minimum EWR, and maximum MRR were determined as the ideal machining performance approach. Since none of the output parameters were prioritized over others, the weights and importances of all targets were taken as “one” (Table 11).
As seen in Fig. 9, the ideal processing parameters for the highest MRR, lowest EWR, and lowest Ra were found to be I = 12.5 A, Ton=66,4242µs, Toff=6µs, and a powder-mixed dielectric. With the selected parameters, the minimum Ra requirement was fulfilled by 38.498%, the minimum EWR requirement was fulfilled by 98.291%, and the maximum MRR requirement was fulfilled by 75.453%. The composite desirability was 65.85%. Due to the direct proportionality between MRR and Ra, low Ra and high MRR could not be achieved at the same time29.
Because specific I, Ton, and Toff values can be selected on the EDM machine where the experiments were performed, the machining parameters for the verification experiment were rounded to the nearest available values. In the final case, the machining parameters were determined as I = 12.5 A, Ton=66 µs, Toff=6 µs, and powder-mixed dielectric. The developed model predicted an MRR of 9.75245 mm3/min, an EWR of 0.0220672 mm3/min, and an Ra of 6.72466 μm. The validation experiment yielded an MRR of 8.06939 mm3/min, an EWR of 0.0188632 mm3/min, and a Ra of 6.805 μm. Accordingly, the developed model predicted MRR with a deviation of −1.68306 mm3/min and a 20.86% error, EWR with a deviation of −0.003204 mm3/min and a 16.99% error, and Ra with a deviation of 0.08034 μm and a 1.18% error (Table 12).
Conclusions
In this study, the optimum machining parameters for the nickel-based alloy “remanium® CSE” (which has not previously been investigated for machinability by EDM) to achieve high MRR, low EWR, and Ra were determined, and the effects of graphite powder addition were investigated. Experiments were conducted using a specially designed setup, using a copper electrode and a graphite powder-mixed dielectric fluid. Graphite powder concentration, current, Ton, and Toff were selected as variable parameters. The findings were evaluated using ANOVA, and a mathematical model was developed using RSM, and the model was validated by conducting validation experiments. The key numerical results and findings obtained from the study are as follows:
-
The highest MRR was measured as 12.667 mm3/min with I = 12.5 A, Ton=99µs, Toff=12µs and powder-mixed dielectric; the lowest MRR was measured as 0.922 mm3/min with I = 3 A, Ton=24µs, Toff=6µs and non-powder-mixed dielectric.
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The most influential parameters on MRR are I, Ton, and powder concentration, respectively. The effect of Toff on MRR is insignificant. It has been found that MRR increases with I, Ton and decreases with Toff.
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The highest EWR was measured as 0.86097 mm3/min with I = 12.5 A, Ton=24µs, Toff=24µs and non-powder-mixed dielectric; the lowest EWR was measured as 0.00545 mm3/min with I = 3 A, Ton=24µs, Toff = 6µs and non-powder-mixed dielectric.
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The most influential parameters on EWR are I and Toff. Ton and powder concentration have a insignificant effect on EWR. EWR has been found to increase as I and Toff increase, and to decrease as Ton increases.
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The lowest Ra was measured as 3.234 μm with I = 3 A, Ton=24µs, Toff=6µs non-powder-mixed dielectric; the highest Ra was measured as 8.931 μm with I = 12.5 A, Ton=99µs, Toff=12µs and non-powder-mixed dielectric.
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The most influential parameters on Ra are I, powder concentration, and Ton, respectively. The effect of Toff on Ra is insignificant.
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Better results were obtained in all performance outputs when powder mixed dielectric was used. On average, MRR increased by 34.54%, EWR decreased by 20.01% and Ra decreased by 12.64% on powder mixed EDM experiments compared to experiments done with same parameters but without powder additive in the dielectric.
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Parameter optimization was performed using the developed model with target outputs of the highest MRR, lowest EWR, and lowest Ra. The model determined the ideal machining parameters as I = 12.5 A, Ton=66µs, Toff=6µs, and a powder-mixed dielectric. According to the validation experiment, the model predicted MRR with a 20.86% error, EWR with a 16.99% error, and Ra with a 1.18% error.
Shaping this metal alloy using EDM provides a superior solution for dentistry, mould-making, and biomedical applications, ensuring high surface quality, minimal electrode wear, and precise machining of complex geometries. Furthermore, the addition of graphite powder significantly increases efficiency and lowers production costs by shortening machining times and reducing electrode wear.
Data availability
Data will be made available upon request. Contact the Corresponding Author if someone wants to request the data from this study.
Abbreviations
- ANOVA:
-
Analysis of variance
- EWR:
-
Electrode wear rate
- I :
-
Discharge current
- MRR:
-
Material removal rate
- Ra :
-
Average surface roughness
- Ton :
-
Pulse-on time
- Toff :
-
Pulse-off time
- RSM:
-
Response surface methodology
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The authors also extend their appreciation to King Saud University for funding the publication of this work through Researchers Supporting Project number (ORF2025R164), King Saud University, Riyadh, Saudi Arabia. This article was co-funded by the European Union under the REFRESH – Research Excellence for Region Sustainability and High-tech Industries project number CZ.10.03.01/00/22_003/0000048 via the Operational Programme Just Transition and has been done in connection with project Students Grant Competition SP2024/087 “Specific Research of Sustainable Manufacturing Technologies” financed by the Ministry of Education, Youth and Sports and Faculty of Mechanical Engineering VŠB-TUO. Article has been done in connection with project Students Grant Competition SP2024/087 “Specific Research of Sustainable Manufacturing Technologies” financed by the Ministry of Education, Youth and Sports and Faculty of Mechanical Engineering VŠB-TUO.
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Concept: Emin Salih San, Hacı Bekir Özerkan, Mehmet SubaşıDesign: Emin Salih San, Robert ČepLiterature: Emin Salih San, Hacı Bekir Özerkan, Mehmet Subaşı, Emre Ayhan, Sachin Salunkhe, Emad S. Abouel Nasr, Robert ČepMethodology: Emre Ayhan, Sachin Salunkhe, Emad S. Abouel Nasr, Robert ČepTesting: Emin Salih San, Hacı Bekir Özerkan, Mehmet Subaşı, Emre Ayhan, Ahmet Mave, Sachin Salunkhe, Emad S. Abouel Nasr, Robert ČepReview: Emin Salih San, Hacı Bekir Özerkan, Mehmet Subaşı, Emre Ayhan, Ahmet Mave, Sachin Salunkhe, Emad S. Abouel Nasr, Robert ČepEditing: Emin Salih San, Hacı Bekir Özerkan, Mehmet Subaşı, Emre Ayhan, Ahmet Mave, Sachin Salunkhe, Emad S. Abouel Nasr, Robert ČepFunding: Emad S. Abouel Nasr, Robert Čep.
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San, E.S., Özerkan, H.B., Subaşı, M. et al. Parametric optimization of graphite powder-mixed electrical discharge machining of Ni-Cr dental alloy by response surface methodology. Sci Rep 15, 44303 (2025). https://doi.org/10.1038/s41598-025-32039-1
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DOI: https://doi.org/10.1038/s41598-025-32039-1











